Determination Of Lead In Gasoline By Extraction And Titration At Kurdistan Region – Iraq

  • Qasim Y. Mohammed MSc. Oil Technology Department, Koya Technical insitiute – Oil technology department – Kurdistan region- Iraq, Babylon university – Babylon - Iraq
  • Sardasht R. Taher MSc. Oil Technology Department, Koya Technical insitiute – Oil technology department – Kurdistan region- Iraq, Babylon university – Babylon - Iraq
  • Hazim Al-Jubury Dr. College of science of women, Koya Technical insitiute – Oil technology department – Kurdistan region- Iraq, Babylon university – Babylon - Iraq
Keywords: Gasoline, Lead, Dual extraction apparatus, TEL, TML

Abstract

A method relates to the determination of lead, tetraethyl lead (TEL) and tetramethyl lead (TML) in commercial gasoline in different places in Kurdistan region – Iraq by dual extraction apparatus and titration was proposed.

References

Thomas, V. M.1995. The elimination of lead in gasoline. Annual Review of Energy and Environment, 20:301-24.

Agency for Toxic Substance and Disease Registry. Case studies in environmental medicine: lead toxicity. U.S. Department of Health and Human Services, 2000.

Ibrahim S.Al-Mutaz and Riyadh N. Furiji, Protection of unleaded gasoline in Riyadh oil refinery, presented at 6th world congress of chemical engineering, Melbourne, Australia, September 23-27, 2001.

Dan, Y.; Dengshan, G.; Gang, Y.; Xianglin, S.; Fan, G and J. Hazard. Mater,An investigation of the treatment of particulate matter from gasoline engine exhaust using non-thermal plasma,Journal of hazardous materials, B127, 149,2005.

Ozaki H.; Watanabe I. and Kuno K., Investigation of the Heavy Metal Sources in Relation to Automobiles,Water, Water, Air, and Soil Pollution. 2004. Volume 157, Issue 1-4, pp 209-223.

Roldan P. S.; Alcantara I. L.; Padilha C. C. F. and Padilha P. M., Determination of copper, iron, nickel and zinc in gasoline by FAAS after sorption and preconcentration on silica modified with 2-aminotiazole groups, Fuel, January – February 2005, Volume 84,Issues 2-3, Pages 305 – 309.

Teixeira L. S. G.; Rocha R. B. S.; Sobrinho E. V.; Guimaraes P. R. B.; Pontes L. A. M. and Teixeira J. S. R., Simultaneous determination of copper and iron in automotive gasoline by X-ray fluorescence after pre-concentration on cellulose paper, Talanta,15 May 2007.Volume 72,Issue 3, Pages 1073 – 1076.

Bezerra M. A.; Santos W. N. L.; Lemos V. A.; Korn M. G. A. and Ferreira S. L. C., On-line system for preconcentration and determination of metals in vegetables by Inductively Coupled Plasma Optical Emission Spectrometry, 5 September 2007. Journal of Hazardous Materials, Volume 148, Issues 1- 2 , Pages 334 – 339.

Amorim F. A. C. and Ferreira S. L. C., Determination of cadmium and lead in table salt by sequential multi-element flame atomic absorption spectrometry. 28 February 2005. Talanta, Volume 65, Issue 4, Pages 960 – 964. [10] Rangar Bye, A simple extraction procedure for the determination of lead in gasoline by atomic absorption spectrometry. 1987. Chem. Edu., 64(2), P188.

Denilson S. S. Santos,; Maria Graças A. Korn, Mauro A. B. Guida, Gabriel L. dos Santos, Valfredo A. Lemos and Leonardo S. G. Teixeira, Determination of copper, iron, lead and zinc in gasoline by sequential multi-element flame atomic absorption spectrometry after solid phase extraction. 2011. J. Braz. Chem. Soc., Vol.22, No.3.

ASTM D2547[13]Indian standard methods of test for petroleum and its products – determination of lead content, 2008.

WHO, Global health risks: Mortality and burden of disease attributable to selected major risks. Geneva, World Health Organization,(2009).

Fewtrell L, Kaufmann R and Pruss-Ustun. Lead: Assessing the environmental burden of disease at national and local levels. Geneva, World Health Organization (Environmental Burden of Disease Series, No. 2; (2003).

UNEP. Draft final review of scientific information on lead. Geneva, United Nations Environment Programme, Chemicals Branch (2008).

Removal of lead from gasoline: technical considerations, Pollution prevention and abatement handbook, World Bank group, July 1998.

Ponadii O.M., Emel’yanov V.E., Oniochenko S.N. and Deineko P.S., Determination of lead in gasoline in the presence of Monomethylaniline, Chemistry and technology of fuels and oils, vol.32,No.3,1996.

Rnald M. and Kenneth C, Extraction of lead from petroleum products eploying aqueous iodine monochloride, United States patent office, patented Dec., 2, 1969.

Methods of test for gasoline: Determination of the high lead content in gasoline by iodine monochloride method, Standarazition organization for G.C.C (GSO), GSO 1087/2002.
Published
2015-04-30
Section
Original Article